引用本文:王晓丽,束平,严海花.4-APP萃取蒸馏法测定地表水中挥发酚的改进[J].环境监控与预警,2010,2(4):21-22
WANG Xiao-li, SHU Ping, YAN Hai-hua.The Improvement of Determining Volatile Phenols in Water by 4-APP Extractive Distillation Method[J].Environmental Monitoring and Forewarning,2010,2(4):21-22
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4-APP萃取蒸馏法测定地表水中挥发酚的改进
王晓丽,束平,严海花
盐城市环境监测中心站,江苏 盐城 224002
摘要:
改进了4-APP萃取蒸馏法测定水中酚的方法,以100mL馏出液代替250mL馏出液,改变了原方法实验过程时间长、费时费力的缺点,特别适合地表水大批量样品的分析。经两种方法测定结果比对,吸光值变化不大,标准曲线相似,回收率符合规范要求;经t检验,测定结果无显著性差异。测定时间南原来的45min缩短至25min左右,大大提高了工作效率。
关键词:  挥发酚  蒸出液  改进
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The Improvement of Determining Volatile Phenols in Water by 4-APP Extractive Distillation Method
WANG Xiao-li, SHU Ping, YAN Hai-hua
Yancheng Environmental Monitoring Central Station,Yancheng,Jiangsu 224002,China
Abstract:
Introduced the improvement of determining volatile phenols in water by 4-APP extractive distillation method. 250 mL distillate was changed to 100 mL to avoid a long time distillation in the original method and can be applied in the analysis of large quantities of surface water samples. According to the comparison of the results of two methods, it showed that little changes were in absorbance, and their standard curves were similar. The recovery of both methods were in line with regulatory requirements. There was no significant difference by t test between the two methods. The distillation time was reduced from 45 min to 25 min. It improved the efficiency greatly.
Key words:  volatile phenols  distillate  improvement