引用本文:陈纯,刘丹,路新燕,李金峰,王琪,申进朝.ASD-ICP-AES 联用快速测定土壤中部分重金属[J].环境监控与预警,2011,3(02):16-20
.A Fast-determination Method of Heavy Metals in Soil by ASD-ICP-AES[J].Environmental Monitoring and Forewarning,2011,3(02):16-20
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ASD-ICP-AES 联用快速测定土壤中部分重金属
陈纯,刘丹,路新燕,李金峰,王琪,申进朝
河南省环境监测中心站,河南 郑州 450004
摘要:
采用样品全自动消解系统对土壤样品进行前处理,采用ICP-AES对土样中的重金属元素一次性测定。通过优化实验,获得土壤中各种重金属的最佳消解条件。结果表明,经优化的消解程序A1能够快速、稳定消解土壤样品,并获得理想测试结果。经检验,ASD-ICP-AES联用的土样测试结果与国际方法测试结果无显著性差异。
关键词:  ASD  消解程序;显著性差异
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A Fast-determination Method of Heavy Metals in Soil by ASD-ICP-AES
Abstract:
Inductive coupled plasma Atomic emission spectrometry (ICP-AES) was used to determine the concentrations of heavy metals in soil, after soil samples were pre-treated by Automated Sample Digestion (ASD) which is the latest equipment for digestion. The best determination results of all kinds of heavy metals in soil can be obtained by choosing the digestion system. Results showed the soil samples can be digested fast and stably by the optimized digestion program A1 and the good determination results can also be obtained. There is no significant differences between the results determined by ASD-ICP-AES and GB standard method.
Key words:  ASD  digestion program  significant difference