土壤中酞酸酯类化合物监测方法的质量控制研究

邓慕<sup>1</sup>; 夏新<sup>2</sup>; 王伟<sup>3</sup>; 马芳<sup>1</sup>; 池靖<sup>2</sup>; 多克辛<sup>3</sup>

引用本文:	邓慕，夏新，王伟，马芳，池靖，多克辛.土壤中酞酸酯类化合物监测方法的质量控制研究[J].环境监控与预警,2012,4(1):14-23
	.The Quality Control in the Monitoring Methods for Phthalate esters in Soil[J].Environmental Monitoring and Forewarning,2012,4(1):14-23

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土壤中酞酸酯类化合物监测方法的质量控制研究
邓慕，夏新，王伟，马芳，池靖，多克辛^1,2,3
1.北京科技大学，北京 100083;2.中国环境监测总站，北京 100012;3.河南省环境监测中心，河南郑州 450004

摘要:

从监测结果控制的角度对近十年的土壤中PAEs监测方法进行了探讨，重点比较了索氏萃取-柱净化-GC/MS、微波萃取-柱净化-GC、加速溶剂萃取-柱净化-GC/MS和加速溶剂萃取-GPC-GC/MS方法的检出限、精密度和准确度。旨在为中国土壤监测方法的建立提供基础支撑，为开展质量控制工作提供评价依据。

关键词: 土壤酞酸酯监测方法质量控制

DOI：

分类号:

基金项目:环保公益性行业科研专项项目（200809140）

The Quality Control in the Monitoring Methods for Phthalate esters in Soil

Abstract:

The monitoring methods for phthalate esters(PAEs) in soil in recent 10 years was discussed from monitoring results control. The detection limit, precision and accuracy between the four monitoring methods including soxhlet extraction-column purification - GC/MS, microwave extraction-column purification-GC, accelerated solvent extraction-column purification-GC/MS and accelerated solvent extraction - GPC - GC/MS method were compared in this study. This paper aimed to provide basic support for the establishment of soil monitoring method, and offer evaluating basis for the conduct of quality control.

Key words: Soil Phthalate Esters Monitoring Method Quality Control