污染土壤中铅的测定方法比对

陈素兰<sup>1; 2</sup>; 王霞<sup>1; 2</sup>; 陈波<sup>1; 2</sup>

引用本文:	陈素兰，王霞，陈波.污染土壤中铅的测定方法比对[J].环境监控与预警,2018,10(5):33-35
	CHEN Su lan，WANG Xia，CHEN Bo.Comparison of Methods for Determination of Lead in Polluted Soil[J].Environmental Monitoring and Forewarning,2018,10(5):33-35

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污染土壤中铅的测定方法比对
陈素兰，王霞，陈波^1,2
1.国家环境保护地表水环境有机污染物监测分析重点实验室，江苏南京 210036;2.江苏省环境监测中心，江苏南京 210036

摘要:

采用原子吸收光谱法(AAS法)、电感耦合等离子发射光谱法(ICP-OES法)和X-荧光光谱法(XRF法)分别测定污染土壤中的铅，并对检出限、精密度、准确度等指标进行了比对。结果表明，3种方法均能满足质量控制的要求，测定结果之间无显著性差异；3种方法中ICP-OES 法和 XRF 法可同时测定多元素，但XRF法更快速简便。

关键词: 铅土壤原子吸收光谱法电感耦合等离子体发射光谱法 X-荧光光谱法

DOI：

分类号:X833；O657.3

文献标识码:B

基金项目:2007年度国家环境保护标准制修订项目（1056）

Comparison of Methods for Determination of Lead in Polluted Soil

CHEN Su lan，WANG Xia，CHEN Bo^1,2

1.State Environmental Protection Key Laboratory of Monitoring and Analysis for Organic Pollutants in Surface Water,Nanjing, Jiangsu 210036,China;2. Jiangsu Environmental Monitoring Center, Nanjing, Jiangsu 210036, China

Abstract:

Atomic Absorption Spectrometry(AAS)，Inductively Coupled Plasma Optical Emission Spectroscopy (ICP-OES) and X-Ray Fluorescence Spectrometry(XRF) were used for determining lead in polluted soil．As compared to the detection limit，precision and accuracy. The results showed that，the three methods could meet the requirement of quality control，there was no significant difference among the determination results．Compared with the method of AAS，ICP-OES and XRF，ICP-OES and XRF method can simultaneously determine multiple elements，but XRF is more rapid and simple.

Key words: Pb Soil Atomic Absorption Spectrometry Inductively Coupled Plasma Optical Emission spectrometry X-Ray Fluorescence Spectrometry