| 引用本文: | WANG Yuan yuan,LU Xin yan,WANG Nan,CHEN Chun,GAO Yong,LIU Dan,PENG Hua.Comparison between Microwave Digestion and Automatic Sample Digestion in the Determination of Heavy Metals in Soil Using ICP-MS[J].Environmental Monitoring and Forewarning,2015,7(5):25~27 |
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| 摘要: |
| 采用微波消解和ASD消解2种消解方式对不同土壤样品进行消解，ICP-MS测定其中重金属含量。微波和ASD2种消解方式均能够较好地提取土壤中的Cr、Co、Ni、Mn和V元素，实验结果的相对误差和相对标准偏差均≤10%，符合实验分析的要求。微波消解精密度优于ASD，可作为优先选择的前处理方法。 |
| 关键词: 微波消解 ASD 土壤 ICP-MS 重金属 |
| DOI： |
| 分类号:O657.3；X833 |
| 文献标识码:B |
| 基金项目:国家仪器科技开发重大专项资助项目（2011YQ060100） |
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| Comparison between Microwave Digestion and Automatic Sample Digestion in the Determination of Heavy Metals in Soil Using ICP-MS |
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WANG Yuanyuan,LU Xinyan,WANG Nan,CHEN Chun,GAO Yong,LIU Dan,PENG Hua
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Henan Environmental Monitoring Center,Zhengzhou,Henan 450004,China
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| Abstract: |
| Soil samples were digested by microwave digestion and automatic sample digestion (ASD) separately,and ICP-MS was used to determine heavy metals in the digestion solution.Both methods were shown well in extracting Cr，Co，Ni，Mn and V in soil,and the relative error and RSD were less than 10%,which were consistent with the requirements for laboratory analysis.The microwave digestion method was shown to have higher precision than the ASD method.Therefore,it was a preferred choice of pretreatment. |
| Key words: Microwave digestion ASD Soil ICP-MS Heavy metal |
