引用本文:袁海勤1,唐松林2,杨旭1,黄文婷1.长江饮用水源地18种挥发性有机物的自动监测应用研究[J].环境监控与预警,2014,6(6):24-26
YUAN Hai qin1,TANG Song lin2,YANG Xu1,HUANG Wen ting1.Study on On line Determination of 18 Volatile Organic Compounds in Drinking Water Source in the Yangtze River[J].Environmental Monitoring and Forewarning,2014,6(6):24-26
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长江饮用水源地18种挥发性有机物的自动监测应用研究
袁海勤1,唐松林2,杨旭1,黄文婷11,2
1.常州市环境监测中心,江苏 常州 213001;2.江苏省环境监测中心,江苏 南京 210036
摘要:
用全自动监测系统测定长江饮用水源地中18种挥发性有机物,通过动态吹扫捕集气相色谱法快速分析水中的挥发性有机物(VOCs),18种有机物的方法检出限为0.07~0.50 μg/L,在0~20 μg/L范围内线性良好,混合标准溶液平行测定的RSD<10%,饮用水样品的加标回收率为72.1%~119.4%。同时,探索了4种监测数据质量控制及质量保证的方法,建立了数据评价体系。
关键词:  长江  饮用水  挥发性有机物  自动监测  气相色谱法
DOI:
分类号:X832
基金项目:江苏省环境监测基金资助项目(1005)
Study on On line Determination of 18 Volatile Organic Compounds in Drinking Water Source in the Yangtze River
YUAN Hai qin1,TANG Song lin2,YANG Xu1,HUANG Wen ting11,2
1.Changzhou Environmental Monitoring Center,Changzhou,Jiangsu 213001,China;2.Jiangsu Environmental Monitoring Center,Nanjing,Jiangsu 210036,China
Abstract:
Automatic determining system was used to determine 18 volatile organic compounds in drinking water source in the YangtzeRiver. VOCs were determined quickly with the gas stripping chromatographic method. The detection limits of 18 volatile organic compounds were between 0.07 and 0.50 μg/L, while the method had a good linearity in the range from 0 to 20 μg/L. The RSD of mixed standard solution was less than 10%.The spike recovery of drinking water samples was 72.1%~119.4%.Four kinds of quality control and quality assurance in monitoring data were explored and the data evaluation system was established
Key words:  Yangtze River  Drinking water  VOCs  Automatic monitoring  Gas chromatography